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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1867591Generated: November 1, 2026

HCID 68565701, compound → HCID 57979565, compound

https://huagongshe.com/reaction/1867591

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68565701HCID 68565701—
CatalystPalladiumHCID 23938—
SolventHydrochloric AcidHCID 313—
SolventEthanolHCID 702—
ProductHCID 57979565HCID 5797956589.7%

Reaction Steps

10% palladium on carbon (10 mg) was added to a solution of 4-benzyl-1-(1-benzylpiperidin-4-yl)imidazolidin-2-one (30 mg, 0.086 mmol) in ethanol (15 mL) and concentrated hydrochloric acid (0.05 mL). The reaction vessel was evacuated and back-filled with nitrogen (3×), then back-filled with hydrogen (40 psi). After 16 h, the mixture was filtered and concentrated to give the title compound (20 mg). MS 260.3 (M+1)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07632832B2
Source datasetuspto-grants-2009_12
ORD IDord-c8c9761e6bd44d6fb873bf290981dcf8
Source noteuspto-grants-2009_12