HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → Phenol, 3-bromo-, 1-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Bromophenol | HCID 11563 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Phenol, 3-bromo-, 1-acetate | HCID 141946 | — |
Reaction Steps
3-bromophenol was dissolved in dichloromethane. Triethylamine (1 eq) and acetic anhydride (2 eq) were added and the mixture was stirred at room temperature for 5 hours. The solvent was eliminated by vacuum evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632870B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-925a0c54b5da44c19aab85d1c2ca7ae4 |
| Source note | uspto-grants-2009_12 |