HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11993208, compound → HCID 11993404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11993208 | HCID 11993208 | — |
| Reactant | HCID 11993403 | HCID 11993403 | — |
| Product | HCID 11993404 | HCID 11993404 | 79.8% |
Reaction Steps
The title compound (36 mg, 79%) as a light yellow foam was prepared from 6-(2-chlorophenyl)-7-(4-chlorophenyl)-3-(4-methoxybicyclo[2.2.1]heptan-1-yl)-[1,2,4]triazolo[4,3-b]pyridazine (Example 17) (47 mg, 0.1 mmol) according to the procedures described for 4-(6-(2-chlorophenyl)-7-(4-chlorophenyl)-[1,2,4]triazolo[4,3-b]pyridazin-3-yl)bicyclo[2.2.2]octan-1-ol (Example 30). HPLC/MS (method A): retention time=3.60 min, (M+H)+=451.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632837B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-616d53b13c7c47b498402990dba22a89 |
| Source note | uspto-grants-2009_12 |