HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → Quinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 15131407 | HCID 15131407 | — |
| Product | Quinoline | HCID 7047 | — |
Reaction Steps
A three-necked flask was charged with 250 ml of toluene, 60 g (0.34 mol) of (2-isocyanatoethyl) 3-chloropropionate obtained in Synthesis Example 2, and 63 g (0.49 mol) of quinoline (boiling point: 237.7° C.), followed by heating at 50° C. for 6 hours with stirring. No acryloyloxyethyl isocyanate was confirmed by gas chromatography analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632965B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-71d253ef34064a82a1da3c70ed8d4018 |
| Source note | uspto-grants-2009_12 |