HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionic Acid → 4-Fluorobenzenesulfonic acid 2-propionyl-aminobenzothiazol-6-yl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionic Acid | HCID 1032 | — |
| Reactant | 4-Fluorobenzenesulfonic acid 2-aminobenzothiazol-6-yl ester | HCID 57980814 | — |
| Reactant | 4-Fluorobenzenesulfonic acid 2-propionylaminobenzothiazol-6-yl ester | HCID 57980824 | — |
| Product | 4-Fluorobenzenesulfonic acid 2-propionyl-aminobenzothiazol-6-yl ester | HCID 86761031 | 93% |
Reaction Steps
According to the method of intermediate 46, 4-fluorobenzenesulfonic acid 2-propionylaminobenzothiazol-6-yl ester is prepared via the action of 4-fluorobenzenesulfonic acid 2-aminobenzothiazol-6-yl ester (intermediate 16, brevetbenzothiazole_V2) with propionic acid. The product, 0.397 g, is obtained in a yield of 93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632952B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-9b93de5158494600bc2bd829b7169940 |
| Source note | uspto-grants-2009_12 |