HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4,5-Trichloropyridine → 3,5-Dichloro-4-{4-[(3,4-dichlorophenyl)sulfonyl]piperidin-1-yl}pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4,5-Trichloropyridine | HCID 3786531 | — |
| Edukt | 4-(3,4-Dichloro-benzenesulfonyl)-piperidine | HCID 22397499 | — |
| Produkt | 3,5-Dichloro-4-{4-[(3,4-dichlorophenyl)sulfonyl]piperidin-1-yl}pyridine | HCID 68550994 | 55% |
Reaktionsschritte
Using the procedure from Example 7A, Step 7E, 4-[(3,4-dichlorophenyl)sulfonyl]piperidine (150 mg, 0.51 mmol) was reacted with 3,4,5-trichloropyridine (224 mg, 1.22 mmol) to afford the title compound (66 mg), a white solid, in 55% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07632838B2 |
| Quelldatensatz | uspto-grants-2009_12 |
| ORD ID | ord-c5eccfd203f24a18baec73a3079b8edb |
| Quellennotiz | uspto-grants-2009_12 |