HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-bromo-2-(trifluoromethyl)- → HCID 68546896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-bromo-2-(trifluoromethyl)- | HCID 9806 | — |
| Reactant | 4-[(4-Tert-butylphenyl)sulfonyl]piperidine | HCID 18538636 | — |
| Product | HCID 68546896 | HCID 68546896 | 17% |
Reaction Steps
Using the procedure from Example 7A, 4-[(4-tert-butylphenyl)sulfonyl]piperidine (100 mg, 0.36 mmol) was reacted with 2-bromobenzotrifluoride (59 μl, 0.43 mmol) to afford the title compound (26 mg), a white solid, in 17% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632838B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-4d337188950d42fca644f6cff6112c99 |
| Source note | uspto-grants-2009_12 |