HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Bromobenzenesulphonyl chloride → HCID 68556406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Reactant | HCID 68553926 | HCID 68553926 | — |
| Product | HCID 68556406 | HCID 68556406 | 97% |
Reaction Steps
Prepared from (2S,4S)-4-(4-fluoro-2-(trifluoromethyl)phenyl)-2-methylpiperidine (120 mg, 0.46 mmol) and 3-bromophenylsulfonyl chloride (99.4 mL, 0.69 mmol) according to scheme III-11 in 97% yield. HRMS: calcd for C19H18BrF4NO2S+H+, 480.02505. found (ESI-FTMS, [M+H]1+), 480.02396.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632838B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-9674f96895fe401fbaf637e8075ebbc4 |
| Source note | uspto-grants-2009_12 |