HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methylaniline → HCID 57982619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methylaniline | HCID 7260 | — |
| Reactant | 2-Chloro-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide | HCID 57982581 | — |
| Product | HCID 57982619 | HCID 57982619 | 54.3% |
Reaction Steps
In a manner similar to Example 243, 2-chloro-4-trifluoromethyl-pyrimidine-5-carboxylic acid cyclohexylmethyl-amide (Example 166a) (50 mg) in 1,4-ioxan (1 ml) and 5-chloro-2-methyl aniline (Aldrich) (110 mg) were reacted to give the title compound (36 mg)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07635701B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-344d373d4a1949f599710a57c031209f |
| Source note | uspto-grants-2009_12 |