HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-(trifluoromethyl)aniline → HCID 57982610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-(trifluoromethyl)aniline | HCID 67960 | — |
| Reactant | HCID 57982687 | HCID 57982687 | — |
| Product | HCID 57982610 | HCID 57982610 | — |
Reaction Steps
2-Chloro-4-trifluoromethyl-pyrimidin-5-carboxylic acid (tetrahydro-pyran-4-ylmethyl)-amide (80 mg) in 2-trifluoromethyl-4-bromoaniline (0.5 ml) was heated at 190° C. under microwave irradiation for 20 minutes. The sample was purified by mass directed auto-purification to afford the title compound (21 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07635701B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-fb4c46170eb94b93bb3b7d9fc85eff07 |
| Source note | uspto-grants-2009_12 |