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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1868440Generated: November 1, 2026

Tert-butyl {[1-(1-ethylcyclobutyl)prop-2-ynyl]oxy}dimethylsilane → 4-{[Tert-butyl(dimethyl)silyl]oxy}-4-(1-ethylcyclobutyl)butanal

https://huagongshe.com/reaction/1868440

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTert-butyl {[1-(1-ethylcyclobutyl)prop-2-ynyl]oxy}dimethylsilaneHCID 85825701—
Reactant4-(1-Butylcyclobutyl) 4-{[tert-butyl(dimethyl)silyl]oxy}butanalHCID 86600163—
SolventEthyl acetate hexaneHCID 21226206—
Product4-{[Tert-butyl(dimethyl)silyl]oxy}-4-(1-ethylcyclobutyl)butanalHCID 86600162—

Reaction Steps

The title compound was prepared according to the procedure described for intermediate 2.6 from tert-butyl {[1-(1-ethylcyclobutyl)prop-2-ynyl]oxy}dimethylsilane. (intermediate 21.5). Rf 0.6 (EtOAc/hexanes 1/4).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07635713B2
Source datasetuspto-grants-2009_12
ORD IDord-1eadf7de9b614503a042f62510e99015
Source noteuspto-grants-2009_12