Cyanuric chloride → HCID 87664814, compound

Participants

Reaction Conditions

Reaction Steps

2.7 g of magnesium was added to 200 ml of tetrahydrofuran and stirred until the magnesium was completely dissolved. To the solution was added dropwise a solution of bromohexadecane (31.1 g) in tetrahydrofuran (200 ml). Thereafter, the resulting solution was heated to 65° C. and reacted for 6 hours with stirring. The reaction solution was slowly added dropwise to a solution of cyanuric chloride (15 g) in tetrahydrofuran (250 ml), and reacted for 12 hours. After completion of the reaction, the resulting solution was evaporated under reduced pressure to obtain a concentrate and then the concentrate was purified by distillation in vacuo to yield pure 2,4-dichloro-6-hexadecyl-1,3,5-triazine.

Provenance & Evidence