HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66968601, compound → HCID 66967948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66968601 | HCID 66968601 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 66967948 | HCID 66967948 | — |
Reaction Steps
The desired compound was prepared from 3-[4-(4-Chloro-benzyl)-piperazin-1-yl]4-hydroxy-pyrrolidine-1-carboxylic acid tert-butyl ester in a manner similar to that described in Example 161. 1H-NMR (300 MHz, DMSO, HCl salt): δ 2.80-3.60 (m, 12 H), 4.20-4.35 (m, 4 H), 7.51 (d, 2 H), 7.66 (d, 2 H). Retention Time (LC, method: Formic acid polar): 0.68 min. MS (M+H+): 296
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07635698B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-f401e2aa31694fdfa66f319e303d7df2 |
| Source note | uspto-grants-2009_12 |