HCID 67099775, compound → HCID 57983400, compound

Participants

Reaction Steps

A mixture of tert-butyl 2-(5-hydroxy-8,8-dimethyl-7-oxo-7,8-dihydroisoquinoline-6-carboxamido)acetate (0.02 g, 0.06 mmol) in 2 mL TFA was stirred at room temperature for 1 hour, M+1=291. The mixture was diluted with 10 mL water. The solution was concentrated and dried to give 0.018 g of the product as a pale yellow solid. MS m/e: (M+H)+ 291.

Provenance & Evidence