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HRID1868925

反应详情

EQUATION

反应方程式

HRID 1868925 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)CNC(=O)C1=C(O)C(C)(C)c2cc(NCCN3CCOCC3)ccc2C1=O
HCID178451294

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)C(O)=C(C(=O)NCC(=O)O)C(=O)c2ccc(NCCN3CCOCC3)cc21
HCID178429101

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=C(O)C(F)(F)F
溶剂HCID6422

未命名化合物

PROCEDURE

实验过程

Tert-butyl 2-(2-hydroxy-1,1-dimethyl-7-(2-morpholinoethylamino)-4-oxo-1,4-dihydronaphthalene-3-carboxamido)acetate (25 mg, 53 μmol) was dissolved in TFA (2 mL) at room temperature for 30 minutes and concentrated to give crude product. The crude product was purified via preparatory TLC to give the title compound. MS (ESI) m/z: Calculated; 417.5: Observed; 418.1.

WORKUP

后处理

  1. concentrationconcentrated
  2. customto give crude product
  3. customThe crude product was purified via preparatory TLC