HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1869144Generated: November 1, 2026
Potassium Carbonate → HCID 86613084, compound
https://huagongshe.com/reaction/1869144
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Chloro-2-chloromethyl-1-propene | HCID 15859 | — |
| Reactant | 4-(3,3-Dichloro-2-propenyloxy)-2,6-dichlorophenol | HCID 11346738 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86613084 | HCID 86613084 | — |
Reaction Steps
20 g of 2,6-dichloro-4-(3,3-dichloro-allyloxy)-phenol and 28.8 g of potassium carbonate are introduced into 150 ml of acetonitrile. 26 g of 3-chloro-2-chloromethyl-propene are then added and the mixture is stirred for 2.5 hours at 80° C. The reaction mixture is cooled to room temperature and filtered, and the filtrate is concentrated. After purification over silica gel, 1,3-dichloro-2-(2-chloromethyl-allyloxy)-5-(3,3-dichloro-allyloxy)-benzene is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07638514B2 |
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| Source dataset | uspto-grants-2009_12 |
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| ORD ID | ord-be3c6a7c067d49e5b5638545b72596bc |
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| Source note | uspto-grants-2009_12 |
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