HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzaldehyde → HCID 57986041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 57986041 | HCID 57986041 | — |
Reaction Steps
Under a nitrogen atmosphere, react 4-chlorobenzaldehyde (14.0 g) and cyclopropylamine (5.7 g) in anhydrous toluene (50 mL) in the presence of molecular sieves for 48 h. Filter the reaction mixture and concentrate the filtrate in vacuo at 60 C to give 4-chlorobenzylidene cyclopropylamine (By as a crystalline solid (15.98 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07638526B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-f9340596a5504910b7ebdd39c40975f1 |
| Source note | uspto-grants-2009_12 |