HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 18695404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,2,4-Trifluoro-5-nitrobenzene | HCID 75012 | — |
| Reactant | Glycine ethyl ester, hydrochloride | HCID 2723640 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18695404 | HCID 18695404 | 20.1% |
Reaction Steps
By using 2.00 g of 2,4,5-trifluoronitrobenzene, 3.43 g of triethylamine, 25 ml of DMF, 25 ml of THF and 1.58 g of glycine ethyl ester hydrochloride, 0.59 g (20%) of N-(4,5-difluoro-2-nitrophenyl)glycine ethyl ester was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06096743 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-3513d2ad17244231b2f8958b66d86ec2 |
| Source note | uspto-grants-2000_08 |