huagongshe.com
HRID1870208

反应详情

EQUATION

反应方程式

HRID 1870208 的结构方程式

REACTANTS

反应物

2
结构：c1c[nH]cn1
HCID795

Imidazole

C3H4N2

结构：CCOC(=O)CNc1cc(F)c(Br)cc1[N+](=O)[O-]
HCID18695448

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CNc1cc(-n2ccnc2)c(Br)cc1[N+](=O)[O-]
HCID18695402

未命名化合物

收率 90.3%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

1.33 (3H, t, J=7.4 Hz), 4.04 (2H, d, J=4.9 Hz), 4.30 (2H, q, J=7.4 Hz), 6.46 (1H, d, J=10.9 Hz), 8.44 (1H, d, J=7.3 Hz), 8.49 (1H, bs). 2) By using 3.36 g (10.5 mmol) of N-(4-bromo-5-fluoro-2-nitrophenyl)glycine ethyl ester, 2.86 g of imidazole and 20 ml of DMF, 3.50 g (90%) of N-[4-bromo-5-(1H-imidazol-1-yl)-2-nitrophenyl]glycine ethyl ester was obtained.