2-Thiophenemethanol → HCID 54470557, compound

Participants

Reaction Steps

2-Chloromethyl-1-isocyanato-3-methylbenzene (2.5 g) and thiophenemethanol (1.57 g) are combined and stirred at RT. When crystallization commences, petroleum ether 50/70 (20 ml) is added and the suspension is stirred for 16 h at RT. After filtration and washing with diethyl ether, 2.57 g (63%) of the title compound are obtained as a solid of m.p. 111-114° C.

Provenance & Evidence