Tripropylamine → HCID 18696299, compound

Participants

Reaction Steps

3.56 g (10 mM) of -1,14-dibromotetradecane are added to 20 ml tripropylamine and held at 80/90° C. over night. The excess tertiary amine is evaporated under vacuum, and a minimal amount of ethanol is added to redissolve the derivative which is reprecipitated with ether. The derivative defined in the title is obtained by recrystallization in a isopropanol/iisopropylic ether mixture, M.P.=170° C.

Provenance & Evidence