HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 18696619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 7-Methoxy-1,2,3,4-tetrahydronaphthalen-1-one | HCID 81276 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18696619 | HCID 18696619 | — |
Reaction Steps
A mixture containing 7-methoxytetralone (25.0 g), benzylamine (15.8 mL), toluene and 4 Å molecular sieves (42.0 g) was heated at reflux for 3.5 h. The mixture was cooled to room temperature, filtered through a layer of Florisil® and concentrated under reduced pressure to yield 42.1 g of crude title compound of Step A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06096895 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-da348ce8b2214c5aacc31e91c5f6c908 |
| Source note | uspto-grants-2000_08 |