Sodium Carbonate → HCID 18692816, compound

Participants

Reaction Steps

N,N-bis(3-hydroxypropyl) aniline (10.46 g) was dissolved in hydrochloric acid (20cm3) at 0-5° C. and sodium nitrite (3.45 g) in water(15cm3) was added dropwise. The mixture was stirred for 1 hr, water (10cm3) was added, made alkaline with sodium carbonate, separated in to an oil and water layer. The oil was dissolved in dichloromethane and the solvent removed to leave N,N-bis(3-hydroxypropyl)4-nitrosoaniline as a yellow solid.

Provenance & Evidence