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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1870799Generated: October 31, 2026

Ethylamine → HCID 86750054, compound

https://huagongshe.com/reaction/1870799

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylamineHCID 6341—
Reactant3-PyridinecarboxaldehydeHCID 10371—
SolventChloroformHCID 6212—
ProductHCID 86750054HCID 86750054—

Reaction Steps

A solution of 3-pyridinecarboxaldehyde (1 g, 9.3 mmol) and ethylamine (661 mg, 10.2 mmol, 70% wt in water) was stirred at room temperature for 18 h. The reaction mixture was diluted with chloroform (20 mL) and dried over anhydrous K2CO3. The solution was filtered and the solvent was evaporated to afford N-(3-pyridylidene)-ethylamine (XVII). 1.15 g (92%), which was used immediately without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06100269
Source datasetuspto-grants-2000_08
ORD IDord-0014fcd27b62469ba6f63acc6effbd13
Source noteuspto-grants-2000_08