HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86755585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 54257618 | HCID 54257618 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86755585 | HCID 86755585 | — |
Reaction Steps
The compound (1.53 g) obtained in Example 51 was dissolved in 1,4-dioxane and methanesulfonic acid (0.27 ml) was added under ice-cooling, after which the solution was stirred for 30 minutes. Subsequently, it was purified by a recrystallization method from 1,4-dioxane to obtain the desired compound (1.89 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100260 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-278b02b9c82c4c15bbcda8142576f4a2 |
| Source note | uspto-grants-2000_08 |