HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromobenzene → HCID 339047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromobenzene | HCID 7961 | — |
| Reactant | Npc164516 | HCID 79038 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 339047 | HCID 339047 | — |
Reaction Steps
The title compound was prepared from bromobenzene (42.1 mL, 0.4 mol), n-butyllithium in hexanes (156 mL, 2.5 M, 0.39 mol) and 8-methyl-8-azabicyclo[3.2.1]-octan-3-one (25 g, 0.18 mol). Yield 14 g (36%), m.p. 157-159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100275 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-ced5be1e975c43838eb928c79f6c66a1 |
| Source note | uspto-grants-2000_08 |