HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl isocyanate → HCID 18694226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl isocyanate | HCID 16035 | — |
| Reactant | Methyl 4'-amino-2'-methyl[1,1'-biphenyl]-4-carboxylate | HCID 21948355 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18694226 | HCID 18694226 | 69.6% |
Reaction Steps
Methyl 4'-amino-2'-methylbiphenyl-4-carboxylate (D2) (1.00 g, 4.1 mmol) and 2-chloroethylisocyanate (0.39 ml, 4.5 mmol) were stirred in dichloromethane (20 ml) for 72 h. The suspension was then diluted with toluene (20 ml), and the solid was filtered off and dried. This gave the title compound (0.99 g, 69%) as a cream solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100272 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-020279eefee143cb96120673600c615a |
| Source note | uspto-grants-2000_08 |