HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 10085156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 10661692 | HCID 10661692 | — |
| Product | HCID 10085156 | HCID 10085156 | — |
Reaction Steps
Following standard procedure C, methyl 2-(4'-nitrophenyl)-1-H-benzimidazole-4-carboxylate was dissolved in liquid ammonia and heated under constant volume in a pressure vessel. The product was purified by column chromatography from dichloromethane/methanol 99:1 and recrystallised from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100283 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-d0c98ff7004d48af9bc07b314dcb5694 |
| Source note | uspto-grants-2000_08 |