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HRID1870958

反应详情

EQUATION

反应方程式

HRID 1870958 的结构方程式

REACTANTS

反应物

2
结构：O=C1C2CC3CC(C2)CC1C3
HCID64151

2-Adamantanone

C10H14O

结构：CC(C)(C)OC(=O)NN
HCID70091

Hydrazinecarboxylic acid, 1,1-dimethylethyl ester

C5H12N2O2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NN=C1C2CC3CC(C2)CC1C3
HCID8039095

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC
溶剂HCID8058

n-Hexane

C6H14

PROCEDURE

实验过程

A hexane solution containing 2-adamantanone (2 g) and tert-butyl carbazate (1.76 g) was heated to reflux for 3 hours. When the solution cooled, the title compound crystallized and was filtered (3.28 g). M.p. 175-177°

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureto reflux for 3 hours
  3. temperatureWhen the solution cooled
  4. customthe title compound crystallized
  5. filtrationwas filtered (3.28 g)