HuagongsheHuagongshe Chemistry Print Report · For research reference only
Adamantanone → N'-(adamantan-2-ylidene)(tert-butoxy)carbohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Adamantanone | HCID 64151 | — |
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N'-(adamantan-2-ylidene)(tert-butoxy)carbohydrazide | HCID 8039095 | — |
Reaction Steps
A hexane solution containing 2-adamantanone (2 g) and tert-butyl carbazate (1.76 g) was heated to reflux for 3 hours. When the solution cooled, the title compound crystallized and was filtered (3.28 g). M.p. 175-177°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100289 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-45dcc2d06d2c4717a52144c574609d78 |
| Source note | uspto-grants-2000_08 |