HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 2-(4-(4-(4-chlorophenyl)-1H-imidazol-1-yl) butyl)-1H-iso indol-1,3(2H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18694800 | HCID 18694800 | — |
| Reactant | HCID 178477960 | HCID 178477960 | — |
| Product | 2-(4-(4-(4-chlorophenyl)-1H-imidazol-1-yl) butyl)-1H-iso indol-1,3(2H)-dione | HCID 70273486 | 37.4% |
Reaction Steps
Using the procedure of Stage A of Example 1, 12.2 g of the product of Stage A, 4.96 g of sodium hydride and 23.83 g of N-4-bromobutyl-phthalamide were reacted to obtain 9.7 g of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100404 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-d8b05194f7ea40b9bb64723494c8af02 |
| Source note | uspto-grants-2000_08 |