HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 4-(4-(Pyridin-3-yl)-1H-imidazol-1-yl)butan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 2-(4-(3-pyridinyl)-1H-imidazol-1-yl)-butyl-1H-iso-indol-1,3(2H)-dione | HCID 18694807 | — |
| Product | 4-(4-(Pyridin-3-yl)-1H-imidazol-1-yl)butan-1-amine | HCID 11042160 | — |
Reaction Steps
Using the procedure of Stage B of Example 1, 1.66 g of the product of Stage A and 0.46 ml of hydrazine hydrate in 30 ml of ethanol were reacted to obtain 936 mg of the desired product which was used as is for the synthesis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100404 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-bbe848dded124a9bb9282cb9a3de561e |
| Source note | uspto-grants-2000_08 |