HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfur dichloride → 3-(Cyclopentyloxy)-4-methoxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfur dichloride | HCID 25353 | — |
| Reactant | 3-(Cyclopentyloxy)-4-methoxybenzoic acid | HCID 2779323 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3-(Cyclopentyloxy)-4-methoxybenzoyl chloride | HCID 2794600 | 98% |
Reaction Steps
54 g of 3-cyclopentyloxy-4-methoxybenzoic acid was added to 30 ml of thiochloride and was stirred for 5 hours. 50 ml of toluene was added to the reaction solution and was concentrated under reduced pressure to obtain 58 g of the dense brown title compound (yield: 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103729 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-2df23536e2ef44cbb85bce58274da44d |
| Source note | uspto-grants-2000_08 |