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HRID1871368

反应详情

EQUATION

反应方程式

HRID 1871368 的结构方程式

REACTANTS

反应物

3
结构：CCCBr
HCID7840

1-Bromopropane

C3H7Br

结构：COc1ccc(C2=NNC(=O)[C@H]3CCCC[C@@H]23)cc1OC
HCID10913208

未命名化合物

结构：CCOc1cc(C2=NNC(=O)[C@H]3CC=CC[C@@H]23)ccc1OC
HCID70003171

未命名化合物

PRODUCTS

生成物

1
结构：CCCN1N=C(c2ccc(OC)c(OC)c2)[C@@H]2CCCC[C@@H]2C1=O
HCID70002226

未命名化合物

PROCEDURE

实验过程

Prepared from compound 1 and 1-bromopropane as described for compound 6. Purified by chromatography (dichloromethane). Crystallized from petroleum ether (60-95° C.). M.p. 95-96° C.

WORKUP

后处理

  1. customPurified by chromatography (dichloromethane)
  2. customCrystallized from petroleum ether (60-95° C.)