HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → (cis)-4-(3,4-Dimethoxyphenyl)-2-(n-propyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 10913208 | — |
| Reactant | (cis)-4-(3-Ethoxy-4-methoxyphenyl)-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one | HCID 70003171 | — |
| Product | (cis)-4-(3,4-Dimethoxyphenyl)-2-(n-propyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70002226 | — |
Reaction Steps
Prepared from compound 1 and 1-bromopropane as described for compound 6. Purified by chromatography (dichloromethane). Crystallized from petroleum ether (60-95° C.). M.p. 95-96° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-3d64a390bbf041479de0a25452255542 |
| Source note | uspto-grants-2000_08 |