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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871377Generated: November 2, 2026

Cyclohexane, (bromomethyl)- → HCID 70003966, compound

https://huagongshe.com/reaction/1871377

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexane, (bromomethyl)-HCID 137636—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70003942—
ProductHCID 70003966HCID 70003966—

Reaction Steps

Prepared from compound 1 and bromomethylcyclohexane as described for compound 8. Purified by chromatography (dichloromethane). Crystallized from petroleum ether (60-95° C.). M.p. 137-139° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-dd5e2bfd88d643d4894a36d4ed8c6976
Source noteuspto-grants-2000_08