HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,6-Dibromohexane → HCID 86755602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,6-Dibromohexane | HCID 12368 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 10913208 | — |
| Product | HCID 86755602 | HCID 86755602 | — |
Reaction Steps
Prepared from compound 1 and 1,6-dibromohexane as described for compound 58. Purified by chromatography [ethyl acetate/petroleum ether (60-80° C.), 1:2]. Crystallized from petroleum ether (60-80° C.). M.p. 74-75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-47bab99ece2647b597d510abfe29c948 |
| Source note | uspto-grants-2000_08 |