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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871388Generated: November 4, 2026

Benzene, (3-bromopropoxy)- → HCID 86755610, compound

https://huagongshe.com/reaction/1871388

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzene, (3-bromopropoxy)-HCID 68522—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70003942—
ProductHCID 86755610HCID 86755610—

Reaction Steps

Prepared from compound 1 and 3-phenoxy-1-bromopropane as described for compound 8. Purified by chromatography (dichloromethane). Crystallized from petroleum ether (60°-80° C.). M.p. 78°-81° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-6ce147bcd8cc48c5826bf0a3872268b9
Source noteuspto-grants-2000_08