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HRID1871403

反应详情

EQUATION

反应方程式

HRID 1871403 的结构方程式

REACTANTS

反应物

3
结构：ClCc1ccccc1
HCID7503

Benzyl chloride

C7H7Cl

结构：COc1ccc(C2=NNC(=O)[C@H]3CC=CC[C@@H]23)cc1OC
HCID10935039

未命名化合物

结构：COc1ccc(C2=NN(Cc3ccccc3)C(=O)[C@H]3CCCC[C@@H]23)cc1OC
HCID70001660

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C2=NN(Cc3ccccc3)C(=O)[C@H]3CC=CC[C@@H]23)cc1OC
HCID11014280

未命名化合物

PROCEDURE

实验过程

Prepared from compound 3 and benzylchloride as described for compound 78. Purified by chromatography [ethyl acetate: petroleum ether (60°-80° C.)/1:3]. Crystallized from diethyl ether. M.p. 133°-135° C.

WORKUP

后处理

  1. customPurified by chromatography [ethyl acetate: petroleum ether (60°-80° C.)/1:3]
  2. customCrystallized from diethyl ether