HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 11014280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | cis-4-(3,4-Dimethoxyphenyl)-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one | HCID 10935039 | — |
| Reactant | (cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70001660 | — |
| Product | HCID 11014280 | HCID 11014280 | — |
Reaction Steps
Prepared from compound 3 and benzylchloride as described for compound 78. Purified by chromatography [ethyl acetate: petroleum ether (60°-80° C.)/1:3]. Crystallized from diethyl ether. M.p. 133°-135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-c668c2e8dd71435691c932ddfa194c8c |
| Source note | uspto-grants-2000_08 |