HRID1871407

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID74234

4-(Chloromethyl)benzoic acid

C8H7ClO2

结构：CCOc1ccc(C2=NNC(=O)[C@H]3CCCC[C@@H]23)cc1OCC

HCID70002320

未命名化合物

结构：COc1ccc(C2=NN(Cc3ccc(C(=O)O)cc3)C(=O)[C@H]3CCCC[C@@H]23)cc1OC

HCID86755615

未命名化合物

PRODUCTS

生成物

结构：CCOc1ccc(C2=NN(Cc3ccc(C(=O)O)cc3)C(=O)[C@H]3CCCC[C@@H]23)cc1OCC

HCID86755616

未命名化合物

PROCEDURE

实验过程

Prepared from compound 7 and 4-chloromethylbenzoic acid as described for compound 83. Purified by chromatography (dichloromethane). Crystallized from diethyl ether. M.p. 152°-154° C.

WORKUP

后处理

customPurified by chromatography (dichloromethane)
customCrystallized from diethyl ether