HRID1871410

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID245650

3-(bromomethyl)benzoic acid

C8H7BrO2

结构：COc1ccc(C2=NNC(=O)[C@H]3CCCC[C@@H]23)cc1OC

HCID10913208

未命名化合物

结构：COc1ccc(C2=NN(Cc3ccc(C(=O)O)cc3)C(=O)[C@H]3CCCC[C@@H]23)cc1OC

HCID86755615

未命名化合物

PRODUCTS

生成物

结构：COc1ccc(C2=NN(Cc3cccc(C(=O)O)c3)C(=O)[C@H]3CCCC[C@@H]23)cc1OC

HCID9866910

未命名化合物

PROCEDURE

实验过程

Prepared from compound 1 and 3-bromomethylbenzoic acid as described for compound 83. Purified by chromatography (ethyl acetate). Crystallized from diethyl ether. M.p. 133°-136° C.

WORKUP

后处理

customPurified by chromatography (ethyl acetate)
customCrystallized from diethyl ether