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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871415Generated: November 3, 2026

3,5-Dimethoxybenzyl chloride → HCID 70002409, compound

https://huagongshe.com/reaction/1871415

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Dimethoxybenzyl chlorideHCID 2758395—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70001660—
ProductHCID 70002409HCID 70002409—

Reaction Steps

Prepared from compound 1 and 3,5-dimethoxybenzylchloride as described for compound 78. Purified by chromatography (dichloromethane). Crystallized from methanol. M.p. 114°-117° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-00b7f9f09fbe47bfb225621b225870d5
Source noteuspto-grants-2000_08