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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871431Generated: November 4, 2026

Phenethyl bromide → HCID 70003823, compound

https://huagongshe.com/reaction/1871431

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenethyl bromideHCID 7666—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70001660—
ProductHCID 70003823HCID 70003823—

Reaction Steps

Prepared from 2-bromoethylbenzene and compound 1 as described for compound 78. Purified by chromatography [ethyl acetate: petroleum ether (60°-80° C.)/1:3]. Crystallized from methanol. M.p. 99°-100° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-c63a4fc6f21f4dd9b76e43acb6f222f4
Source noteuspto-grants-2000_08