huagongshe.com
HRID1871440

反应详情

EQUATION

反应方程式

HRID 1871440 的结构方程式

REACTANTS

反应物

3
结构：ClC/C=C/c1ccccc1
HCID639658

(E)-Cinnamyl chloride

C9H9Cl

结构：COc1ccc(C2=NNC(=O)[C@H]3CCCC[C@@H]23)cc1OC
HCID10913208

未命名化合物

结构：COc1ccc(C2=NN(Cc3ccccc3)C(=O)[C@H]3CCCC[C@@H]23)cc1OC
HCID70001660

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C2=NN(C/C=C/c3ccccc3)C(=O)[C@H]3CCCC[C@@H]23)cc1OC
HCID86755630

未命名化合物

PROCEDURE

实验过程

Prepared from compound 1 and 3-phenyl-2-[trans]propenylchloride as described for compound 78. Purified by chromatography (dichloromethane). Crystallized from diethyl ether at -20° C. M.p. 76°-79° C.

WORKUP

后处理

  1. customPurified by chromatography (dichloromethane)
  2. customCrystallized from diethyl ether at -20° C