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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871440Generated: November 2, 2026

Cinnamyl chloride → HCID 86755630, compound

https://huagongshe.com/reaction/1871440

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCinnamyl chlorideHCID 639658—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-2-Benzyl-4-(3,4-dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70001660—
ProductHCID 86755630HCID 86755630—

Reaction Steps

Prepared from compound 1 and 3-phenyl-2-[trans]propenylchloride as described for compound 78. Purified by chromatography (dichloromethane). Crystallized from diethyl ether at -20° C. M.p. 76°-79° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-2a39334b8b274491b4b9808cf4079732
Source noteuspto-grants-2000_08