HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Benzyloxy)-2-(chloromethyl)benzene → (cis)-4-(3,4-Dimethoxyphenyl)-2-(2-benzyloxybenzyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Benzyloxy)-2-(chloromethyl)benzene | HCID 563507 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 10913208 | — |
| Product | (cis)-4-(3,4-Dimethoxyphenyl)-2-(2-benzyloxybenzyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70003457 | — |
Reaction Steps
Prepared from compound 1 and 2-benzyloxybenzylchloride as described for component 78. Purified by chromatography [ethyl acetate/petroleum ether (60°-80° C.), 1:3]. M.p. colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-fbd8e85655094d3c8d5da0814da40927 |
| Source note | uspto-grants-2000_08 |