HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Hydrochloric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 53949543 | HCID 53949543 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 86755635 | HCID 86755635 | — |
Reaction Steps
Reaction and post-treatment were carried out according to Example 4 using 353 mg of ethyl 3-[4-[2-[[1-(4-biphenylyl)ethylidene]aminoxy]ethoxy]phenyl]-2-(N-phenyl-N-ethylamino)propionate obtained in Example 11 and 2 ml of a 1N aqueous sodium hydroxide solution. The product thus obtained was further treated with a 4N hydrogen chloride-dioxane solution to obtain 280 mg of hydrochloride of the desired compound as an amorphous powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103907 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-e6fc2e734a284265b32e69d1d52421f3 |
| Source note | uspto-grants-2000_08 |