Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | Cyclohexene | HCID 8079 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | CID 15879360 | HCID 15879360 | — |
Reaction Steps
Dissolve cyclohexene (9.035 g, 0.11 mol) in tetrahydrofuran (3 mL) and cool to -15° C. Slowly add borane (24.1 mL of a 2.3M solution in tetrahydrofuran) and stir at -15° C. for 1 hour to give dicyclohexylborane (55 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06107275 |
|---|
| Source dataset | uspto-grants-2000_08 |
|---|
| ORD ID | ord-0ed1f5fb3bba463db583563dc7673682 |
|---|
| Source note | uspto-grants-2000_08 |
|---|
