Borane → CID 15879360

HRID 1871879Notes

Reaction equation

HRID 1871879 reaction equation
[CH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.[BH3:7]>O1CCCC1>[CH:1]1([BH:7][CH:1]2[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 6331BoraneHCID 8079Cyclohexene

Product 1

HCID 15879360CID 15879360

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent2×

Conditions

Temperature
-15 °C

Procedure

Dissolve cyclohexene (9.035 g, 0.11 mol) in tetrahydrofuran (3 mL) and cool to -15° C. Slowly add borane (24.1 mL of a 2.3M solution in tetrahydrofuran) and stir at -15° C. for 1 hour to give dicyclohexylborane (55 mmol).

Sources & evidence

ORD record
ord-0ed1f5fb3bba463db583563dc7673682
Source dataset
uspto-grants-2000_08
Patent number
US06107275

Reaction notes

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